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Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide

M. M., Yusoff and Reibenspies, Joseph H. and Talaty, Erach R. (1997) Synthesis and X-ray Analysis of (RS)-N-tert-butyl-2-anilino- 3,3-dimethylbutanamide. Journal of Chemical Crystallography, 27 (12). pp. 727-730. ISSN 1074-1542 (print), 1572-8854 (online)

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Abstract

The crystal and molecular structure of (RS)-N-Tert-butyl-2-anilino-3,3-dirnethylbutanamide, a derivative of an amino acid that was obtained by highly selective cleavage of 1,3-di-tert-butylaziridinone by aniline, is described. The racemic mixture of the amide crystallizes in the space grot)p P 2in with four molecules per unit cell. Crystal Data: a - 10.483(2) A, h - 6.206(I) A, c = 24.767(5) A, [3 - 90.39(3), V = 1611.5(6) A ~, R(F)[I > 2r = 0.0679, wR(F 2) [1 > 2or(l)] = 0. 1148.

Item Type: Article
Additional Information: Please click to official URL. 3 citations. IF: 0.513
Uncontrolled Keywords: Crystal structure; Selectivity in ring-opening of an aziridinone
Subjects: Q Science > Q Science (General)
Q Science > QD Chemistry
Faculty/Division: Faculty of Industrial Sciences And Technology
Depositing User: Prof. Dr. Mashitah Mohd Yusoff
Date Deposited: 25 Feb 2014 06:44
Last Modified: 22 Jan 2018 01:39
URI: http://umpir.ump.edu.my/id/eprint/4772
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