Norhayati, Abdullah and M. Z., Yahya and R. A., mahmod and Gupta, Arun (2018) Full factorial design analysis approach for preparation of poly(HEMA-co-EGDMA-co- VBC) microsphere particles. In: 4th International Conference Of Chemical Engineering And Industrial Biotechnology (ICCEIB 2018) , 1-2 Aug 2018 , Seri Pacific Hotel, Kuala Lumpur. pp. 563-564..
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Full factorial design analysis approach for preparation of poly(HEMA-co-EGDMA-co- VBC) microsphere particles.pdf Download (638kB) | Preview |
Abstract
The application of a more reliable full factorial experiment has not been well-explored in studies of crosslinked polymer synthesis. In this paper, statistically full factorial design experimental was explored in the study of poly(HEMA-co-EGDMA-co-VBC) synthesis via suspension polymerization. Three independent factors, i.e. monomer concentration (HEMA), amount of crosslinker (EGDMA) and amount of co-monomer (VBC) were investigated to study the effect and interaction factors on morphology and yield of terpolymer particles in 23 factorial design of experiments. The percentage of EGDMA was found to be the most significant factor affecting the morphology of particle, with good quality particles obtained when the percentage of EGDMA increasing. Meanwhile, the factorial analysis suggests that all of the factors show a significant effect on particles yield, with more than 80% yield obtained when all factors was increased.
| Item Type: | Conference or Workshop Item (Lecture) |
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| Uncontrolled Keywords: | Full factorial design; microsphere particles; DoE; crosslinked polymer; statistical analysis |
| Subjects: | T Technology > TP Chemical technology |
| Faculty/Division: | Faculty of Chemical & Natural Resources Engineering |
| Depositing User: | Mrs. Neng Sury Sulaiman |
| Date Deposited: | 10 Jan 2019 03:37 |
| Last Modified: | 10 Jan 2019 03:37 |
| URI: | http://umpir.ump.edu.my/id/eprint/23722 |
| Download Statistic: | View Download Statistics |
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