Nuramira Fateha, Sukor and Rohayu, Jusoh and Nur Syahirah, Kamarudin (2021) Intensification of phenolic acids extraction from Aleppo oak via probe type sonication method: Kinetic, antioxidant and cost evaluation. Chemical Engineering Research and Design, 166. pp. 227-236. ISSN 0263-8762. (Published)
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Abstract
This work aimed to evaluate the optimum conditions for efficient extraction of phenolic acids, namely gallic acid (GA) and tannic acid (TA) from Aleppo oak by ultrasonic-probe assisted extraction (UPAE) method. Furthermore, an extensive study on kinetic, antioxidant activity and cost evaluation aspects in comparison with classical hydro-distillation extraction (CHDE) method was also examined. Sonication demonstrated a superior effect on the extraction of target compounds in which the UPAE method was seven times more efficient compared to the classical hydro-distillation extraction (CHDE) method. Result revealed that under optimized optimum condition of 40% duty cycle and 70 °C extraction temperature, GA and TA were yielded at 870.90 ± 0.03 mg GAE/g and 3157.97 ± 0.05 mg TAE/g, respectively. Kinetic analysis affirmed the extraction rate as controlling factor in extracting phenolic acids. Strong antioxidant activity was observed at a IC50, 26.57 ± 0.03 μg/mL. Besides, the cost assessment study indicates that the extraction process requires US$ 0.25 and US$ 0.06 per mg/g extracts produced for CHDE and UPAE, respectively. Notably, findings revealed that UPAE method is four-fold more cost-effective compared to the CHDE method, providing a new direction for extracting active compounds from complex plants.
Item Type: | Article |
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Uncontrolled Keywords: | Ultrasonic-probe assisted extraction, Aleppo oak, Rate law, Antioxidant activity, Cost evaluation |
Subjects: | T Technology > TP Chemical technology |
Faculty/Division: | Institute of Postgraduate Studies Faculty of Chemical and Process Engineering Technology |
Depositing User: | Dr. Rohayu Jusoh |
Date Deposited: | 12 May 2022 07:19 |
Last Modified: | 12 May 2022 07:19 |
URI: | http://umpir.ump.edu.my/id/eprint/34077 |
Download Statistic: | View Download Statistics |
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