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Synthesis, crystal structure and Hirshfeld surface analysis.pdf Available under License Creative Commons Attribution. Download (5MB) | Preview |
DOI/Official URL: https://doi.org/10.1016/j.cdc.2023.101064
Abstract
Ethyl 4 hydroxy-2-(4-hydroxyphenyl)-1-methyl-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate, C14H15NO5 (1) was synthesized via multicomponent reaction (MCR) of sodium diethyl oxalacetate, methylamine, and 4-hydroxybenzaldehyde. The structure of 1 was elucidated by using FT-IR, NMR and GCMS. These results were further confirmed by means of single crystal X-ray crystallography. The results showed that 1 was crystallized in orthorhombic space group Pca21 where a = 17.102(4), b = 9.923(2), c = 16.037(4), Å. The quantification of intermolecular interactions in the crystal structure was obtained by Hirshfeld surface analysis and showed that the H•••H contacts were the most dominant interactions.
| Item Type: | Article |
|---|---|
| Additional Information: | Indexed by Scopus |
| Uncontrolled Keywords: | 2,3-Dioxopyrrolidine; Crystal structure; Hirshfeld surface analysis; Multicomponent reaction; Pyrrolone |
| Subjects: | H Social Sciences > HD Industries. Land use. Labor Q Science > Q Science (General) T Technology > T Technology (General) |
| Faculty/Division: | Faculty of Industrial Sciences And Technology |
| Depositing User: | Mr Muhamad Firdaus Janih@Jaini |
| Date Deposited: | 28 May 2024 08:10 |
| Last Modified: | 28 May 2024 08:10 |
| URI: | http://umpir.ump.edu.my/id/eprint/40949 |
| Download Statistic: | View Download Statistics |
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