Raj, K. R. and Sunarti, Abd Rahman (2019) Preliminary fractional factorial design (FFD) study using incorporation of graphene oxide in PVC in mixed matrix membrane to enhance CO2 /CH4 separation. In: IOP Conference Series: Materials Science and Engineering; 1st Process Systems Engineering and Safety Symposium 2019, ProSES 2019 , 4 September 2019 , Kuantan, Pahang, Malaysia. pp. 1-15., 702 (012041). ISSN 1757-8981
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Preliminary fractional factorial design (FFD) study using incorporation of graphene oxide in PVC in mixed matrix membrane.pdf Available under License Creative Commons Attribution. Download (1MB) | Preview |
Abstract
Mixed matrix membranes (MMMs) comprising of where polyvinyl chloride (PVC) and graphene oxide (GO) were employed in the membrane fabrication in order to improve the membrane characteristics. In this study of gas separation using mixed matrix membrane, gases such as CO2 and CH4 were used. The objectives of this research were to synthesize and develop MMMs PVC/GO, and also to carry out screening to determine best factors condition for membrane to function at high selectivity. The development of MMMs PVC/GO was based on 5 factors. Based on the screening tests, the run which was made up of factors PVC 20%, GO 4%, 1 bar of pressure during gas permeation, NMP solvent, and immersion time of 300s, shows to have the highest selectivity at 26.09 which was above the upper bound lines in the Robeson's Upper bound plot. Fractional Factorial Design (FFD) was applied to study the minimalization of influenced factors during MMMs preparation. Based on the FFD run, the R-squared (R2) was 1.00. Factors that had less impact on the maximum selectivity were the time membrane immersed in water bath (s), and also gas pressure during gas permeation test.
| Item Type: | Conference or Workshop Item (Lecture) |
|---|---|
| Additional Information: | Indexed by Scopus |
| Uncontrolled Keywords: | Fractional factorial designs; Gas permeation tests; High selectivity; Maximum selectivity; Membrane characteristics; Membrane fabrication; Mixed matrix membranes; Polyvinyl chloride (PVC) |
| Subjects: | Q Science > QD Chemistry T Technology > T Technology (General) T Technology > TP Chemical technology |
| Faculty/Division: | Institute of Postgraduate Studies Faculty of Chemical and Process Engineering Technology |
| Depositing User: | Mr Muhamad Firdaus Janih@Jaini |
| Date Deposited: | 24 May 2023 04:15 |
| Last Modified: | 24 May 2023 04:15 |
| URI: | http://umpir.ump.edu.my/id/eprint/35877 |
| Download Statistic: | View Download Statistics |
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