Preparation of AC/TiO2 doped N-Ce synthesized via microwave irradiation for amoxicillin photodegradation

Nur Athirah Awatif, Abdul Rahman and Azduwin, Khasri and Noor Hasyierah, Mohd Salleh and Mohd Ridzuan, Mohd Jamir and Nur Hidayah, Mat Yasin (2024) Preparation of AC/TiO2 doped N-Ce synthesized via microwave irradiation for amoxicillin photodegradation. International Journal of Integrated Engineering, 16 (2). pp. 237-244. ISSN 2229-838X. (Published)

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Abstract

Activated carbon (AC) supported with titanium dioxide (TiO2) doped with Nitrogen (N) and Cerium (Ce) were synthesized for adsorption and photodegradation of amoxicillin antibiotic. Optimization of the modified AC/TiO2 composite was developed for removal amoxicillin from aqueous solution using sol-gel method assisted with microwave radiation under UV Light. In this work, four variables were optimized via Central Composite Design (CCD) under Response Surface Methodology (RSM) and they were urea (N source) (A: 0.02 g – 0.2 g), cerium (III) nitrate hexahydrate (Ce source) (B: 0.02 g – 0.2 g), activated carbon dosage (C: 0.1 g – 0.5 g) and microwave power (D: 600 W – 800 W) to observe amoxicillin degradation. Under optimum variables preparation, results indicated that the modified AC/TiO2 photocatalyst prepared with 0.5 g activated carbon, doped with 0.02 g urea and 0.2 g cerium exhibited 93.6 % amoxicillin removal under UV light.

Item Type: Article
Additional Information: Indexed by Scopus
Uncontrolled Keywords: Activated carbon; Amoxicillin; optimization; Photodegradation; Titanium dioxide
Subjects: T Technology > TP Chemical technology
Faculty/Division: Faculty of Chemical and Process Engineering Technology
Depositing User: Mrs. Nurul Hamira Abd Razak
Date Deposited: 06 Jun 2025 01:35
Last Modified: 06 Jun 2025 01:35
URI: http://umpir.ump.edu.my/id/eprint/44729
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